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Trace Element Determination in Sulfur Samples Using a Novel Digestion Bomb Prior to ICP-MS Analysis
Yin, Xuebo1,3; Wang, Xiaoyuan1,2,3; Chen, Shuai1,3; Ma, Yao1,3; Kun, Guo1,4; Zeng, Zhigang1,2,3
2018-07-01
发表期刊ATOMIC SPECTROSCOPY
ISSN0195-5373
卷号39期号:4页码:137-141
通讯作者Wang, Xiaoyuan(wangxiaoyuan@qdio.ac.cn)
摘要A method has been developed for the ICP-MS determination of trace elements in sulfur samples using a novel closed digestion bomb with a double inner arc seal design. The method is simple, precise, and accurate, completely digests the sulfur sample, and allows for the determination of the trace elements Ba, C,e, Cd, Co, Cr, Cs, Dy, Er, Eu, Ga, Gd, Ho, La, Li. Pb, Pr, Rb, Sm, Sr, Tb, Tm, U, V, Y, and Yb. Upon the addition of trace element standards to a high purity sulfur chemical reagent, the recoveries were 91.5% for La to 109.7% for U. The detection limits of this method were 1.49 ng g(-1) for Sr to 0.009 ng g(-1) for Tm and Lu.
收录类别SCI
语种英语
资助项目National Natural Science Foundation of China[41476044] ; National Natural Science Foundation of China[41706052] ; Chinese Academy of Sciences[133137KYSB20170003] ; Special Fund for the Taishan Scholar Program of Shandong Province[ts201511061] ; Qingdao National Laboratory for Marine Science and Technology[2015ASTP-0S17] ; Aoshan Talents Program ; National Natural Science Foundation of China[41476044] ; National Natural Science Foundation of China[41706052] ; Chinese Academy of Sciences[133137KYSB20170003] ; Special Fund for the Taishan Scholar Program of Shandong Province[ts201511061] ; Qingdao National Laboratory for Marine Science and Technology[2015ASTP-0S17] ; AoShan Talents Program
WOS研究方向Spectroscopy
WOS类目Spectroscopy
WOS记录号WOS:000444821000001
出版者PERKIN-ELMER CORP
引用统计
被引频次:11[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.qdio.ac.cn/handle/337002/160193
专题海洋地质与环境重点实验室
通讯作者Wang, Xiaoyuan
作者单位1.Chinese Acad Sci, Inst Oceanol, Key Lab Marine Geol & Environm, Qingdao 266071, Peoples R China
2.Qingdao Natl Lab Marine Sci & Technol, Lab Marine Mineral Resources, Qingdao 266071, Peoples R China
3.Chinese Acad Sci, Ctr Ocean Mega Sci, Qingdao 266071, Peoples R China
4.Shandong Univ Sci & Technol, Coll Earth Sci & Engn, Qingdao 266590, Peoples R China
第一作者单位中国科学院海洋研究所
通讯作者单位中国科学院海洋研究所
推荐引用方式
GB/T 7714
Yin, Xuebo,Wang, Xiaoyuan,Chen, Shuai,et al. Trace Element Determination in Sulfur Samples Using a Novel Digestion Bomb Prior to ICP-MS Analysis[J]. ATOMIC SPECTROSCOPY,2018,39(4):137-141.
APA Yin, Xuebo,Wang, Xiaoyuan,Chen, Shuai,Ma, Yao,Kun, Guo,&Zeng, Zhigang.(2018).Trace Element Determination in Sulfur Samples Using a Novel Digestion Bomb Prior to ICP-MS Analysis.ATOMIC SPECTROSCOPY,39(4),137-141.
MLA Yin, Xuebo,et al."Trace Element Determination in Sulfur Samples Using a Novel Digestion Bomb Prior to ICP-MS Analysis".ATOMIC SPECTROSCOPY 39.4(2018):137-141.
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