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Iron-catalyzed alkynylation of tertiary aliphatic amines with 1-iodoalkynes to synthesize propargylamines
Ma, Lina1,2,3; Shi, Xiaolin1,2,3; Li, Xiaowei1,2,3; Shi, Dayong1,2,3
2018-12-21
Source PublicationORGANIC CHEMISTRY FRONTIERS
ISSN2052-4129
Volume5Issue:24Pages:3515-3519
Corresponding AuthorShi, Dayong(shidayong@qdio.ac.cn)
AbstractA method of alkynylation of tertiary aliphatic amines with 1-iodoalkynes has been developed in the presence of FeCl2 as a catalyst and tert-butyl hydroperoxide as an oxidant. With this method, a variety of propargylamines were obtained in good to excellent yields from inexpensive and readily available reagents. The studies on the possible reaction pathway suggest that this reaction proceeds through a radical process.
DOI10.1039/c8qo01028e
Indexed BySCI
Language英语
Funding ProjectCPSF-CAS Joint Foundation for Excellent Postdoctoral Fellows[2017LH024] ; National Natural Science Foundation of China[81773586] ; National Natural Science Foundation of China[81703354] ; Key Research and Development Project of Shandong Province[2016GSF201193] ; Key Research and Development Project of Shandong Province[2016ZDJS07A13] ; Key Research and Development Project of Shandong Province[2016GSF115002] ; Key Research and Development Project of Shandong Province[2016GSF115009] ; Key Research Program of Frontier Sciences, CAS[QYZDB-SSW-DQC014] ; Shandong Provincial Natural Science Foundation for Distinguished Young Scholars[JQ201722] ; National Program for Support of Top-notch Young Professionals ; Taishan Scholar Youth Project of Shandong Province ; Project of Discovery, Evaluation and Transformation of Active Natural Compounds, Strategic Biological Resources Service Network Program of the Chinese Academy of Sciences[ZSTH-026]
WOS Research AreaChemistry
WOS SubjectChemistry, Organic
WOS IDWOS:000452114300003
PublisherROYAL SOC CHEMISTRY
Citation statistics
Document Type期刊论文
Identifierhttp://ir.qdio.ac.cn/handle/337002/155797
Collection实验海洋生物学重点实验室
Corresponding AuthorShi, Dayong
Affiliation1.Chinese Acad Sci, Inst Oceanol, Key Lab Expt Marine Biol, Qingdao 266071, Peoples R China
2.Qingdao Natl Lab Marine Sci & Technol, Lab Marine Drugs & Bioprod, Qingdao 266237, Peoples R China
3.Univ Chinese Acad Sci, Beijing 100049, Peoples R China
First Author AffilicationKey Laboratory of Experimental Marine Biology, Institute of Oceanology, Chinese Academy of Sciences
Corresponding Author AffilicationKey Laboratory of Experimental Marine Biology, Institute of Oceanology, Chinese Academy of Sciences
Recommended Citation
GB/T 7714
Ma, Lina,Shi, Xiaolin,Li, Xiaowei,et al. Iron-catalyzed alkynylation of tertiary aliphatic amines with 1-iodoalkynes to synthesize propargylamines[J]. ORGANIC CHEMISTRY FRONTIERS,2018,5(24):3515-3519.
APA Ma, Lina,Shi, Xiaolin,Li, Xiaowei,&Shi, Dayong.(2018).Iron-catalyzed alkynylation of tertiary aliphatic amines with 1-iodoalkynes to synthesize propargylamines.ORGANIC CHEMISTRY FRONTIERS,5(24),3515-3519.
MLA Ma, Lina,et al."Iron-catalyzed alkynylation of tertiary aliphatic amines with 1-iodoalkynes to synthesize propargylamines".ORGANIC CHEMISTRY FRONTIERS 5.24(2018):3515-3519.
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