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Iron-catalyzed alkynylation of tertiary aliphatic amines with 1-iodoalkynes to synthesize propargylamines
Ma, Lina1,2,3; Shi, Xiaolin1,2,3; Li, Xiaowei1,2,3; Shi, Dayong1,2,3
2018-12-21
发表期刊ORGANIC CHEMISTRY FRONTIERS
ISSN2052-4129
卷号5期号:24页码:3515-3519
通讯作者Shi, Dayong(shidayong@qdio.ac.cn)
摘要A method of alkynylation of tertiary aliphatic amines with 1-iodoalkynes has been developed in the presence of FeCl2 as a catalyst and tert-butyl hydroperoxide as an oxidant. With this method, a variety of propargylamines were obtained in good to excellent yields from inexpensive and readily available reagents. The studies on the possible reaction pathway suggest that this reaction proceeds through a radical process.
DOI10.1039/c8qo01028e
收录类别SCI
语种英语
资助项目CPSF-CAS Joint Foundation for Excellent Postdoctoral Fellows[2017LH024] ; National Natural Science Foundation of China[81773586] ; National Natural Science Foundation of China[81703354] ; Key research and development project of Shandong province[2016GSF201193] ; Key research and development project of Shandong province[2016ZDJS07A13] ; Key research and development project of Shandong province[2016GSF115002] ; Key research and development project of Shandong province[2016GSF115009] ; Key Research Program of Frontier Sciences, CAS[QYZDB-SSW-DQC014] ; Shandong Provincial Natural Science Foundation for Distinguished Young Scholars[JQ201722] ; National Program for Support of Top-notch Young Professionals ; Taishan scholar Youth Project of Shandong province ; Project of Discovery, Evaluation and Transformation of Active Natural Compounds, Strategic Biological Resources Service Network Program of the Chinese Academy of Sciences[ZSTH-026] ; CPSF-CAS Joint Foundation for Excellent Postdoctoral Fellows[2017LH024] ; National Natural Science Foundation of China[81773586] ; National Natural Science Foundation of China[81703354] ; Key Research and Development Project of Shandong Province[2016GSF201193] ; Key Research and Development Project of Shandong Province[2016ZDJS07A13] ; Key Research and Development Project of Shandong Province[2016GSF115002] ; Key Research and Development Project of Shandong Province[2016GSF115009] ; Key Research Program of Frontier Sciences, CAS[QYZDB-SSW-DQC014] ; Shandong Provincial Natural Science Foundation for Distinguished Young Scholars[JQ201722] ; National Program for Support of Top-notch Young Professionals ; Taishan Scholar Youth Project of Shandong Province ; Project of Discovery, Evaluation and Transformation of Active Natural Compounds, Strategic Biological Resources Service Network Program of the Chinese Academy of Sciences[ZSTH-026]
WOS研究方向Chemistry
WOS类目Chemistry, Organic
WOS记录号WOS:000452114300003
出版者ROYAL SOC CHEMISTRY
引用统计
被引频次:7[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.qdio.ac.cn/handle/337002/155796
专题实验海洋生物学重点实验室
通讯作者Shi, Dayong
作者单位1.Chinese Acad Sci, Inst Oceanol, Key Lab Expt Marine Biol, Qingdao 266071, Peoples R China
2.Qingdao Natl Lab Marine Sci & Technol, Lab Marine Drugs & Bioprod, Qingdao 266237, Peoples R China
3.Univ Chinese Acad Sci, Beijing 100049, Peoples R China
第一作者单位实验海洋生物学重点实验室
通讯作者单位实验海洋生物学重点实验室
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GB/T 7714
Ma, Lina,Shi, Xiaolin,Li, Xiaowei,et al. Iron-catalyzed alkynylation of tertiary aliphatic amines with 1-iodoalkynes to synthesize propargylamines[J]. ORGANIC CHEMISTRY FRONTIERS,2018,5(24):3515-3519.
APA Ma, Lina,Shi, Xiaolin,Li, Xiaowei,&Shi, Dayong.(2018).Iron-catalyzed alkynylation of tertiary aliphatic amines with 1-iodoalkynes to synthesize propargylamines.ORGANIC CHEMISTRY FRONTIERS,5(24),3515-3519.
MLA Ma, Lina,et al."Iron-catalyzed alkynylation of tertiary aliphatic amines with 1-iodoalkynes to synthesize propargylamines".ORGANIC CHEMISTRY FRONTIERS 5.24(2018):3515-3519.
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